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Knowledge Base

Testing for Fipronil?

Testing eggs for Fipronil contaminationAre you looking to test for Fipronil insecticide contamination in eggs?

 

Fipronil is a popular insecticide used to treat pets with fleas. The World Health Organization (WHO) considers Fipronil to be moderately toxic and notes very large quantities can cause damage to certain organs, including the kidney, liver and thyroid glands.

 

A Fipronil & Metabolite Standards Kit and individual standards are now available through Kinesis from
AccuStandard Inc.

Fipronil & Metabolite testing standards kitThe Fipronil and Metabolite range includes: FipronilFipronil SulfoneFipronil SulfideFipronil Desulfinyl. These can be purchased together in one kit as listed below, or as individual standards as required.

 

We have also published a new application note where SPE (Solid Phase Extraction) and QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) Sample Preparation Methods are compared for the extraction and clean-up of Fipronil from egg samples.

Download the application note: Detection of Fipronil in Egg Samples by LC-MS/MS by following the link at the bottom of this page.

 

Click the 'Add to Basket' link below to start your order.

FIPRONIL AND METABOLITE TESTING KIT
Kit Part No. Contains Description Volume Concentration SDS Order Online
P-FIP-MET-KIT P-738S-A Fipronil 1 mL 100 µg/mL in Acetone View Add to Basket
  P-780S-A Fipronil Sulfone 1 mL 100 µg/mL in Acetone    
  P-781S-A Fipronil Sulfide 1 mL 100 µg/mL in Acetone    
  P-782S-A Fipronil Desulfinyl 1 mL 100 µg/mL in Acetone    

 

FIPRONIL AND METABOLITE INDIVIDUAL STANDARDS
Part No. Description CAS No. Volume Category Concentration SDS Order Online
BIOC-229N-10MG Fipronil 120068-37-3 10 mg Biocides Neat View  Add to Basket
P-738N Fipronil 120068-37-3 10 mg Herb./Pest. Neat View  Add to Basket
P-738S Fipronil 120068-37-3 1 mL Herb./Pest. 100 µg/mL 
in Methanol
View  Add to Basket
P-738S-A Fipronil 120068-37-3 1 mL Herb./Pest. 100 µg/mL 
in Acetone
View  Add to Basket
P-780S-A Fipronil Sulfone 120068-36-2 1 mL Herb./Pest. 100 µg/mL
in Acetone
View  Add to Basket
P-781N-5MG Fipronil Sulfide 120067-83-6 5 mg Herb./Pest. Neat View  Add to Basket
P-781S-A Fipronil Sulfide 120067-83-6 1 mL Herb./Pest. 100 µg/mL
in Acetone
View  Add to Basket
P-782S-A Fipronil Desulfinyl 205650-65-3 1 mL Herb./Pest. 100 µg/mL
in Acetone
View  Add to Basket

 

SAMPLE PREPARATION
Part No. Description Pack Size Order Online
MS-LN0202 Cleanert LipoNo QuEChERS, 200mg/2ml PK/100 Add to Basket
MS-LN0415 Cleanert LipoNo QuEChERS, 400mg/15ml PK/50 Add to Basket
PE0603X Cleanert PEP Plus, 60mg/3ml PK/50 Add to Basket
PE2003X Cleanert PEP Plus, 200mg/3ml PK/50 Add to Basket
PE1506X Cleanert PEP Plus, 150mg/6ml PK/30 Add to Basket
PE2006X Cleanert PEP Plus, 200mg/6ml PK/30 Add to Basket
ESF-NY-13-022 KX Syringe Filter, Nylon, 13mm, 0.22μm PK/100 Add to Basket

 

LC-MS/MS COLUMN
Part No. Description Pack Size Order Online
UO930503-0 Unisol C18, 3 μm 5cm x 3mmid PK/1 Add to Basket

 

Kinesis Application Note: Detection of Fipronil in Egg Samples by LC-MS/MS

In this Application Note, SPE (Solid Phase Extraction) and QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) Sample Preparation Methods was compared for the extraction and clean-up of Fipronil from egg samples. The subsequent analysis was performed using LC-MS/MS. Initially, Fipronil was extracted from egg samples using 1%, v/v, acetic acid in acetonitrile and the two sample preparation methods, SPE (using Cleanert PEP Plus) and QuEChERS (using Cleanert LipoNo), then compared. The analysis was carried out using a Unisol C18 3μm 5cm x 3mmid HPLC Column. The results show recoveries greater than 70% at concentrations of 4μg/kg and RSDs lower than 5%.

Download the application note now by clicking the thumbnail below.

    Detection of Fipronil in Egg Samples by LC-MS/MS

    0.27 MB

    Date posted: 23rd Aug 2017 , 4:21pm